Apparatus for evaporating fluid materials



ug. 24, 1943. R. R. HAUGH 2,327,889

I APPARATUS FOR EVAPORATING LUID MATERIALS* Filed Dec. 1e, 1959 Ja J6 7J j Z0 14 3 l fj- J6 l l I( n Z J7'j i jf I 'l a l l', 2 [1], im I) 'I at?" a l f 27 77- I. I 25 /7 79:5

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I .72 Il x 6 r l. A l V 7@ V 9 I Z5-venan ozu j bzwmJ Patented Aug. 24, 1943 UNITED vSTATE s PATENT .i olfrlcrs i APPARATUS non EVAPORATING FLUID MATERIALS Raymond R. Haugh, Chicago, Ill.,` assignor to Vernon Usher, Chicago, lll. V l

Application December 1e, 19st, serial No. soassof l" 1 claim, (o1. 15a-4.)

rIhis invention relatesV to a method andifapparatus for evaporating fluid materials and,` more particularly to the drying of milk, eggs, and other food products. l 1.,

One object ofqthisinvention' is to provide 'for rapid evaporation `of liquids at relativelylowiiavor of the milk. A furthenobject is tofprovide for the dryingvof yeastwithout the .destruction of any substantial portion of the cells thereof. Still a further object is to provide means for treating fluids With superhc-eatedsteam.V Other features and advantages will beapparent from the rfollowing specification and drawing,l `in Whichv y I Figure 1 is a side elevationalvieW of apparatus embodying Amy invention, With the covering insulationtl'iereforV shown in section; Figure `2,is a detail fragmentary sectional View of the upper portion of the apparatus; and Figure 3 is a detail sectional View of the portion of the apparatus indicated by the lines 3--3 of Figure l. j

Although .my apparatus may be used for vany purpose in Whichit is desired to obtain the rapid drying of a` liquid while maintaining the same at a low temperature, it is particularly adapted inthe product being more readily re-constitutedfrk The apparatus is also suitable in the drying of pumpkin iiour, carrot flour, bananaA ilour,`al1 Vegetable `and cereal flours,fruit flours,` meat Y flours, meat juices, andV combinations of these substances -yvith other materials such as sugar, salt, and the like. Milk andcream, howevenare particularly adaptedV for use ,With` this apparatus.l

If the milk or cream is combinedwith glucose or syrup, the keeping qualities of the resultant product 4are greatly enhanced, and, in addition, the product may be dissolved or re-constituted much more readilythan products of this type which )have ,heretofore been made.

It surely that the ready soiubiiny andthe,-

ability tobe easily re-constituted are due to several factors. n 'Iheuse of allow temperature and high. vacuum tend to prevent; any substantial changes in the material.V The prevention `of `local heating eifects, as is possible withl my apparatus,

' is also helpful. Even morefimportant isthe fact that indrying aV liquid ahighly viscousor plastic mass is formedas the'drying progresses.` `When the` material is in such condition, ythe further evaporation or `drying causes the formation of bubblesof vapormwithin thematerialand this in turn produces expansion within the material.

Because the material .isalready inthe form of a plastic masshsubstantiallyno `foaming will resulta Neverthelessvi',l as the drying;` nears completion, the bubbles of vapor formed in the material produce small interstitial air spaces therein and for the drying of milk, eggsyeafS i'/, yand similar table juices, bacterial cultures or other products Where the live organism is to be retained in the iinished product.L The materials to be dried `are preferably in the fluid form and may be sprayed into the apparatus. During the evaporation in vacuum, the solids `Which are produced are expanded into porous particles, in which condition they are easily and readily re-constituted to their original condition When treated with a suitabl amount of Water.

Before the drying operation is completed, the materials may be combined With a viscous liquid such as glucose or malt syrup or the like. `The addition of these substances aids in the expansion of the product being dried, which, in turn, results result ina highly soluble product- The addition ofv glucose orvmalt syrup tothe mixturefnotonly serves to aid inpreserving the product, but also helps in the formation of the plastic mass.' l p `In, the drying ofmilk vby ordinarylmethods, care must betakenr ofiburningv or charting, the milkas a result ofthegmilkuoming in 'contact with heated `metal surfaces or due local heating effects. In other words, vvlfienmthe container-,'is

heated to. a temperature in excessofthe temperaturefof the milk, themilkimmediately adjacent the walls of the container maybe burned. To a certain extent this may be avoided by oper-` ating the apparatus under a reduced pressure and at a lower tern perature-` Howeventhe use of- Vacuum in the evaporation of a quantity of liquid usuallymeans that considerable diilculty will be encountered because of the foaming and effervescence of the liquid. By means of my invention I have succeeded in quickly raising the temperature of the milk without encountering difficulty from burning or foaming.

In the specific embodiment of my invention described herein, a container I of any suitable size and shape provides a mixing chamber I I and has in addition an. enlarged lower portion I2 adapted to receive material after treatment. The outer surface of the container Ill is preferably provided with insulation 23.

The container I D is equipped with' an aperture I3 which communicates with the upper end of the container. An upper extension. I4 of the container IIJ may threadedly engage the mounting I5 to which is secured the T-shaped pipe IISA communicating with the aperture I3. The pipe I6 has at one end an opening Il, at whiclrpoint the pipe may be connected to a conduit or pipe I8 which leads to any suitable source of vacuum (not shown). of flexible material. The other end I9 of the pipe I6 is so arranged as to permit a uid inlet pipe 20 to pass therethrough. 'A closure member 2l, engaging the nuid inlet pipe 20 and the end ofthe' pipe I6, provides an-air-ti'ght seal around theinlet pipe.

-' The'inlet'p'ipe 2B is preferably equipped with aA nozzle-F22 providing a small y-oriice through which liquids orvflu`ids may be sprayed.Y Iriorder to obtain-'a dispersement 'ofthe fluid into smallparticles when passing through the noz,-l

zle 22, the fluidis preferably placed under pres- 'sureiin the-inletpipeZU. A

"Spaced away'from thefapertureA I 35 and rvthe-inlet' pipe -2Il is an inlete23 adapted to permit the now into the container of superheated steam. If desired, lan electrical heating element 214 may be mountedon a" support-25 behind aV filter or screen 26 land connected to a source of electrical 'l energy bythe Wires 21 and 28. In the lower portion of the container-a gate valve 29'of any suitableconstruction=may-be used to remove materiallfromthe'containenl Inoperation, the' 'uid -toy be evaporated or driedis passed into thejcontainer I6 through the inlet pipeZ," being sprayed'f'rom the'nozzle 22.

.At'the Sametime 'thefinletpipe ZE'at-thebase of ,the mixing chamber I-I furnishes a constant flow of superhea-ted -steamforother heating medium.

lWhen steam is` used it is usually preferred that it-be heated to a temperaturebetween-350"and '4.60"V I'. However,v ifv `the operation is carried out at larreduced pressure, for example, one-half atmosphere, steam' superheated lto. onlyl 1759- 200F.maybe-use'd. g fi "The container" is subjected to evacuation through the conduit I8 lane'taperture I3. In this manner thefcontainer is under a reduced pressure when thergaseusfheating medium and the fluid fluidl to dryness.

it is possible to readily heat and evaporate the The steam does not condense in any substantial quantities, but is' merely desuperheated, or in other Words, reduced in tem.. perature to the boiling point of Water ai; the particular pressure under which the system is rbeing operated. In the event that any of the steam k is condensed as, a result ofitscontact-.with the fluid-spray,v it is again` quickly vaporized by the inflow'of additional superheated steam.

Foaming and elervesence is normally caused by the formation of large bubbles of vapor in a relativelylargebody of liquid and particularly if'the liquid has a high viscosity. .In my procv` If desired, the conduit I8 may be.V

ess, since the steam is brought into contact with the liquid while the liquid is dispersed in the form of nely divided particles, this disadvantage is eliminated.

The conditions of time, temperature and pressure will, of course, vary somewhat with the different. materials which mayY beevaporatedffor dried. In'the drying 'of yeastandeggsior'exe ample, I prefer .to use a much lower. temperature and pressure than for the treatment oimilkiw' 'Aspreviously stated, the, materials yto'be dried, such as milk and eggs, may, if: desired,y be mixed with .other substances such asrour and glucose or syrup before treatment.'i Onthe other llzalnitl,l

all of-y these materials, .includingyeash iff thisis to -be dried, shouldbe in a uidcondition .inorder 'thatthe apparatus 'described'. herein. may vvbe used.4 However;l if they: are: not .-in..uid condi.-I tion.' itjmeansfonly that they cannot ,be sprayed' into the mixing chamber. I

While there 'are showmandfdescribed certain embodiments .of thevinvention, .it i'sV to. be under- Y- stood that it is capable'bf many.ino'dications;y

Changes, therefore, intheconstruction and ar- ,I rangement may be made Without departingfrom the spirit and'scope of the'invention as disclosed inthe appendedclaim,- in' Which'itfig intended to claim allv novelty? inherent :rin'fthe invention as broadly as permissible, vin view of the priorart.

I claim: und Apparatus of the lcharacter describedforthe evaporation ofiluids, AWhichcomprises ac'ontain'- er, an outlet 'conduit at-thef'upper'end-of said' container, fan.l inlet'v pipe positionedv withiny said outlet conduit,'said inlet pipe being provided with* a` small orifice adapted to produce'a lfluid spray,

another inlet in 'said container, Isaid 'second inlet being spaced'vaway Vfrom saidrst-mentioned inlet and being' adapted to permitA the 'introduction' of superheated steam into thecontainer, a screen Within said *cntainerextendingabout said sec. ond inlet i andlf/'forming a "chamber thereabo'ut,v

heater means in said container for heatingfth'e steam introduced':through said rsecond inlet, anv

outlet in the lower portion o fythe` container for removing solids or'liquids thererom,`an d means connected with said outletconduit for evacuating said container whereby vthe superheated steam introduced through said second-inlet passes upwardly through the container toI saidoutletcon fis. ..1 l f 1 -1 vmlYMoNn RHAUGH. 

